化工社化工社 化学情報印刷レポート · 研究参考用
Acrolein → N-(4-Chlorobenzylidene)-4-methylthioaniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acrolein | HCID 7847 | — |
| 反応物 | alpha-(4-Chlorophenyl)-alpha-(4-methylthioanilino)acetonitrile | HCID 21862778 | — |
| 生成物 | N-(4-Chlorobenzylidene)-4-methylthioaniline | HCID 21862850 | — |
反応手順
Following a procedure similar to that described in Example 21(iii), but using α-(4-chlorophenyl)-α-(4-methylthioanilino)acetonitrile [prepared as described in step (ii) above] and acrolein as starting materials, the title compound was obtained as an orange-colored powder (yield 32%), melting at 203-205° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | USRE039420E1 |
| 出典データセット | uspto-grants-2006_12 |
| ORD ID | ord-e8566af10da04d4cb67722f52d006b8e |
| 出典メモ | uspto-grants-2006_12 |