P-Anisidine → 4-Methoxy-N-(4-sulfamoylbenzylidene)aniline

反応式

[S:1]([C:5]1[CH:12]=[CH:11][C:8]([CH:9]=O)=[CH:7][CH:6]=1)(=[O:4])(=[O:3])[NH2:2].[CH3:13][O:14][C:15]1[CH:21]=[CH:20][C:18]([NH2:19])=[CH:17][CH:16]=1>>[CH3:13][O:14][C:15]1[CH:21]=[CH:20][C:18]([N:19]=[CH:9][C:8]2[CH:11]=[CH:12][C:5]([S:1](=[O:4])(=[O:3])[NH2:2])=[CH:6][CH:7]=2)=[CH:17][CH:16]=1

参加物

反応物 2

HCID 7732P-Anisidine

HCID 1510884-Sulfamoylbenzaldehyde

生成物 1

HCID 218627504-Methoxy-N-(4-sulfamoylbenzylidene)aniline

実験手順

Following a procedure similar to that described in Example 1(i), but using 4-sulfamoylbenzaldehyde and 4-methoxyaniline as starting materials, the title compound was obtained as a pale yellow powder (yield 85%).

出典と根拠

ORDレコード: ord-6cb093e6962e45fdb092374e34d44826
出典データセット: uspto-grants-2006_12
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: USRE039420E1

反応ノート

読み込み中…