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Strontium nitrate → Strontium bis(o-ethyl 3,5-di-tert-butyl-4-hydroxybenzylphosphonate)
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Strontium nitrate | HCID 24848 | — |
| 反応物 | Sodium (o-ethyl 3,5-di-tert-butyl-4-hydroxybenzylphosphonate) | HCID 86587835 | — |
| 生成物 | Strontium bis(o-ethyl 3,5-di-tert-butyl-4-hydroxybenzylphosphonate) | HCID 86587834 | — |
反応手順
ml aqueous solution of 317 mg (1.5 mmol) strontium nitrate was added dropwise to 7.5 ml aqueous solution of 1 g (2.85 mmol) sodium (o-ethyl 3,5-di-tert-butyl-4-hydroxybenzylphosphonate) (phosphorus compound C described above) at room temperature under stirring. After the mixture was stirred for 1 hour, the precipitates were separated by filtration, washed with water and dried to give strontium bis(o-ethyl 3,5-di-tert-butyl-4-hydroxybenzylphosphonate), 513 mg (48 %).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07144614B2 |
| 出典データセット | uspto-grants-2006_12 |
| ORD ID | ord-01e8315078304df19cb80ab97cdd960f |
| 出典メモ | uspto-grants-2006_12 |