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Barium nitrate → HCID 86587836、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Barium nitrate | HCID 24798 | — |
| 反応物 | Sodium (o-ethyl 3,5-di-tert-butyl-4-hydroxybenzylphosphonate) | HCID 86587835 | — |
| 生成物 | HCID 86587836 | HCID 86587836 | — |
反応手順
5 ml aqueous solution of 392 mg (1.5 mmol) barium nitrate was added dropwise to 7.5 ml aqueous solution of 1 g (2.85 mmol) sodium (o-ethyl 3,5-di-tert-butyl-4-hydroxybenzylphosphonate) (phosphorus compound C described above) at room temperature under stirring. After the mixture was stirred for 1 hour, the precipitates were separated by filtration, washed with water and dried to give barium bis(o-ethyl 3,5-di-tert-butyl-4-hydroxybenzylphosphonate), 508 mg (45%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07144614B2 |
| 出典データセット | uspto-grants-2006_12 |
| ORD ID | ord-09e335155be044908b5cd50c70a075a6 |
| 出典メモ | uspto-grants-2006_12 |