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HRID 856868作成日:2026年10月26日

Barium nitrate → HCID 86587836、化合物

https://huagongshe.com/reaction/856868

反応式

関与物質

役割名称HCID仕込み量
反応物Barium nitrateHCID 24798—
反応物Sodium (o-ethyl 3,5-di-tert-butyl-4-hydroxybenzylphosphonate)HCID 86587835—
生成物HCID 86587836HCID 86587836—

反応手順

5 ml aqueous solution of 392 mg (1.5 mmol) barium nitrate was added dropwise to 7.5 ml aqueous solution of 1 g (2.85 mmol) sodium (o-ethyl 3,5-di-tert-butyl-4-hydroxybenzylphosphonate) (phosphorus compound C described above) at room temperature under stirring. After the mixture was stirred for 1 hour, the precipitates were separated by filtration, washed with water and dried to give barium bis(o-ethyl 3,5-di-tert-butyl-4-hydroxybenzylphosphonate), 508 mg (45%).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07144614B2
出典データセットuspto-grants-2006_12
ORD IDord-09e335155be044908b5cd50c70a075a6
出典メモuspto-grants-2006_12