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Cesium Chloride → 2-Chloro-4-[6-(4-trifluoromethyl-phenyl)-pyrimidin-4-yloxy]-benzothiazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cesium Chloride | HCID 24293 | — |
| 反応物 | 4-[6-(4-Trifluoromethyl-phenyl)-pyrimidin-4-yloxy]-benzothiazol-2-ylamine | HCID 10091650 | — |
| 触媒 | Cuprous chloride | HCID 62652 | — |
| 生成物 | 2-Chloro-4-[6-(4-trifluoromethyl-phenyl)-pyrimidin-4-yloxy]-benzothiazole | HCID 10476517 | — |
反応手順
The title compound was prepared in an analogous manner to the conditions of Example 91 by reacting 4-[6-(4-trifluoromethyl-phenyl)-pyrimidin-4-yloxy]-benzothiazol-2-ylamine (Example 65) with CsCl and CuCl. MS (ESI, pos. ion.) m/z: 408 (M+1).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07144888B2 |
| 出典データセット | uspto-grants-2006_12 |
| ORD ID | ord-d5a40e3dd74b44f0bbeb53c35f3a7969 |
| 出典メモ | uspto-grants-2006_12 |