P-Anisidine → N-4-methoxyphenyl-N'-cyano-O-phenylisourea
反応式
C1C=CC(O[C:8]([O:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[N:9][C:10]#[N:11])=CC=1.[CH3:19][O:20][C:21]1[CH:27]=[CH:26][C:24]([NH2:25])=[CH:23][CH:22]=1>C(O)(C)C>[CH3:19][O:20][C:21]1[CH:27]=[CH:26][C:24]([NH:25][C:8](=[N:9][C:10]#[N:11])[O:12][C:13]2[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=2)=[CH:23][CH:22]=1参加物
4
実験手順
A slurry of diphenyl cyancarbonimidate (1 g) in isopropanol (10 mL) was treated with 4-methoxyaniline (517 mg). After stirring at room temperature for a further 2.5 hours the reaction mixture was filtered. The insoluble material was washed with isopropanol to give the title compound (778 mg) as a white solid, which was used without further purification.
後処理
- filtrationwas filtered
- washThe insoluble material was washed with isopropanol
出典と根拠
- ORDレコード
- ord-c5d16a2e556b4d6f8942453347cd673f
- 出典データセット
- uspto-grants-2006_12
- 特許番号
- US07148215B2
反応ノート
読み込み中…