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Benzene, 1-bromo-3-ethyl- → 6-(3-ethylphenethyl)-6-cyclopentyl-dihydro-3H-pyran-2,4-dione
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzene, 1-bromo-3-ethyl- | HCID 123170 | — |
| 反応物 | 4-Bromo-2-fluoro-1-(1-methylethyl)benzene | HCID 21051092 | — |
| 反応物 | 6-(2-Cyclopentyl-2-hydroxy-but-3-ynyl)-2,2-dimethyl-[1,3]dioxin-4-one | HCID 22499802 | — |
| 生成物 | 6-(3-ethylphenethyl)-6-cyclopentyl-dihydro-3H-pyran-2,4-dione | HCID 16076108 | — |
反応手順
The title compound was prepared analogously to Example A(64), where 1-Bromo-3-ethyl-benzene was substituted in place of 4-bromo-2-fluoro-1-isopropylbenzene in that example, and Enantiomer A of 6-(2-cyclopentyl-2-hydroxybut-3-ynyl)-2,2-dimethyl-4H-1,3-dioxin-4-one was used in place of the racemic alkyne.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07148226B2 |
| 出典データセット | uspto-grants-2006_12 |
| ORD ID | ord-0b04e3c1de6247ecbb5d5e7b2e0266b9 |
| 出典メモ | uspto-grants-2006_12 |