2,4,6-Cycloheptatrien-1-one, 2-methoxy-7-(5-pyrimidinyl)- → 2,4,6-Cycloheptatrien-1-one, 2,3,5,7-tetrakis(acetyloxy)-

反応式

COC1C(=O)C(C2C=NC=NC=2)=CC=CC=1.COC1C(=O)C(C2C=NC=NC=2)=CC=CC=1.[CH3:33][C:34]([O:36][C:37]1[CH:44]=[C:43]([O:45][C:46]([CH3:48])=[O:47])[C:41](=[O:42])[C:40]([O:49][C:50]([CH3:52])=[O:51])=[C:39]([O:53][C:54]([CH3:56])=[O:55])[CH:38]=1)=[O:35].COC1C(=O)C(C2C=NC=NC=2)=CC=CC=1>>[CH3:33][C:34]([O:36][C:37]1[CH:44]=[C:43]([O:45][C:46]([CH3:48])=[O:47])[C:41](=[O:42])[C:40]([O:49][C:50]([CH3:52])=[O:51])=[C:39]([O:53][C:54]([CH3:56])=[O:55])[CH:38]=1)=[O:35]

参加物

反応物 2

HCID 106562462,4,6-Cycloheptatrien-1-one, 2-methoxy-7-(5-pyrimidinyl)-

HCID 131726171SP11 SP12 SP11

生成物 1

HCID 140190602,4,6-Cycloheptatrien-1-one, 2,3,5,7-tetrakis(acetyloxy)-

実験手順

If a negative result is obtained in this step SP12, the dialog control part 63 returns to step SP11, and then, it repeats the loop of steps SP11-SP12-SP11 until an affirmative result is obtained in this step SP12.

後処理

customan affirmative result

出典と根拠

ORDレコード: ord-8a47b68d5d024c229b59a3784760480c
出典データセット: uspto-grants-2006_12
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07152050B2

反応ノート

読み込み中…