化工社化工社 化学情報印刷レポート · 研究参考用
Prenderol → 5,5-Diethyl-2-(4-nitrobenzyl)-1,3,2-dioxaphosphorinan-2-oxide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Prenderol | HCID 8284 | — |
| 反応物 | (4-Nitro-benzyl)-phosphonic acid | HCID 5180708 | — |
| 生成物 | 5,5-Diethyl-2-(4-nitrobenzyl)-1,3,2-dioxaphosphorinan-2-oxide | HCID 18928100 | — |
反応手順
4-Nitrobenzylphosphonic acid and 2,2-diethyl-1,3-propanediol were treated in the same manner as in Reference Example 20 to yield 5,5-diethyl-2-(4-nitrobenzyl)-1,3,2-dioxaphosphorinan-2-oxide, which was then recrystallized from ethanol-hexane to yield colorless prisms having a melting point of 159°-160° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05716944 |
| 出典データセット | uspto-grants-1998_02 |
| ORD ID | ord-fda0ac62c8d74173872038bd0fdd5d72 |
| 出典メモ | uspto-grants-1998_02 |