化工社化工社 化学情報印刷レポート · 研究参考用
2-Fluorobenzophenone → (2-Fluorophenyl)(phenyl)methanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Fluorobenzophenone | HCID 67650 | — |
| 反応物 | Sodium borohydride | HCID 4311764 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | (2-Fluorophenyl)(phenyl)methanol | HCID 10584252 | 99% |
反応手順
2-Fluorobenzophenone (15.0 g) is dissolved in ethanol and sodium borohydride (3.8 g) is added in portions and the mixture is stirred for 20 hours. The reacted solution is concentrated under reduced pressure and extracted with chloroform and water to give crude (2-fluorophenyl)phenylmethanol (15.0 g) (quantitative) as colorless liquid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05716950 |
| 出典データセット | uspto-grants-1998_02 |
| ORD ID | ord-c9141cfb5aeb445e97fcde16004fb780 |
| 出典メモ | uspto-grants-1998_02 |