ホームMCPワークベンチSkills
ホームワークベンチ通知マイページ
llms.txt · MCPガイドプライバシーポリシー · 利用規約 · サポートv1.8.0
  1. ホーム
  2. /反応

Water → 5-Bromo-4-chloro-2-methoxymethoxybenzyl cyanide

HRID 862072
ノート
印刷プレビュー

反応式

HRID 862072 の反応式
[Br:1][C:2]1[C:3]([Cl:14])=[CH:4][C:5]([O:10][CH2:11][O:12][CH3:13])=[C:6]([CH:9]=1)[CH2:7]O.[CH2:15]([N:17](CC)CC)C.CS(Cl)(=O)=O.O>ClCCl>[Br:1][C:2]1[C:3]([Cl:14])=[CH:4][C:5]([O:10][CH2:11][O:12][CH3:13])=[C:6]([CH:9]=1)[CH2:7][C:15]#[N:17]
参加物実験手順後処理出典と根拠反応ノート

参加物

6

反応物 4

HCID 962WaterHCID 8471TriethylamineHCID 31297Methanesulfonyl chlorideHCID 106128525-Bromo-4-chloro-2-methoxymethoxybenzyl alcohol

生成物 1

HCID 107559665-Bromo-4-chloro-2-methoxymethoxybenzyl cyanide

試薬・触媒・溶媒 1

HCID 6344Dichloromethane溶媒2 回

実験手順

To a solution of 5-bromo-4-chloro-2-methoxymethoxybenzyl alcohol (137.9 g) and triethylamine (105 ml) in dichloromethane (500 ml) was added at 0° C. methanesulfonyl chloride (45.5 ml) over a period of 30 minutes. The mixture was stirred overnight (13 hours), while warming up to room temperature. The reaction mixture was poured into water, to which was added dichloromethane for extraction. The extract solution was dried (anhydrous magnesium sulfate) and concentrated. To a suspension of the concentrate and sodium cyanide (51.4 g) in dichloromethane (40 ml) was added dropwise at 0° C. DMSO (300 ml). The mixture was then stirred for 3 hours at room temperature. The reaction mixture was poured into water, which was subjected to extraction with ethyl acetate. The extract solution was washed with water, dried (anhydrous magnesium sulfate) and concentrated. The concentrate was purified by means of a silica gel column chromatography (eluted with ethyl acetate/hexane) to give 5-bromo-4-chloro-2-methoxymethoxybenzyl cyanide (86.4 g) (Compound B-35). The physical properties are shown in [Table 6].

後処理

  1. extractionfor extraction
  2. dry with materialThe extract solution was dried (anhydrous magnesium sulfate)
  3. concentrationconcentrated
  4. additionTo a suspension of the
  5. concentrationconcentrate
  6. additionsodium cyanide (51.4 g) in dichloromethane (40 ml) was added dropwise at 0° C
  7. stirringThe mixture was then stirred for 3 hours at room temperature
  8. additionThe reaction mixture was poured into water, which
  9. extractionwas subjected to extraction with ethyl acetate
  10. washThe extract solution was washed with water
  11. dry with materialdried (anhydrous magnesium sulfate)
  12. concentrationconcentrated
  13. customThe concentrate was purified by means of a silica gel column chromatography (eluted with ethyl acetate/hexane)

出典と根拠

ORDレコード
ord-7d98c758b67442c79ad3cadb8fb5f9d7
出典データセット
uspto-grants-1998_02
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US05716971

反応ノート

読み込み中…

このページの内容参加物実験手順後処理出典と根拠反応ノート