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1-(4-Methoxyphenyl)-1-phenylmethanamine → N-(4-Methoxybenzhydryl)-3-cyanoandrosta-3,5-diene-17beta-carboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-(4-Methoxyphenyl)-1-phenylmethanamine | HCID 350041 | — |
| 反応物 | S-2pyridyl 3-cyanoandrosta-3,5-diene-17beta-thiocarboxylate | HCID 15380265 | — |
| 生成物 | N-(4-Methoxybenzhydryl)-3-cyanoandrosta-3,5-diene-17beta-carboxamide | HCID 15380278 | 82% |
反応手順
Following a procedure similar to that described in Example 3(b), but using S-2-pyridyl 3-cyanoandrosta-3,5-diene-17β-thiocarboxylate [prepared as described in Example 3(a)] and 4-methoxybenzhydrylamine (prepared as described in Preparation 15) as starting materials, in relative proportions similar to those used in that Example, the title compound was obtained in a yield of 82%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05717088 |
| 出典データセット | uspto-grants-1998_02 |
| ORD ID | ord-c2a34d67a5194413a758f91ca4cafa9d |
| 出典メモ | uspto-grants-1998_02 |