化工社化工社 化学情報印刷レポート · 研究参考用
2-Propenoic acid, 3-phenyl- → 1-Indanone, 3-phenyl-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Propenoic acid, 3-phenyl- | HCID 8784 | — |
| 反応物 | Aluminum(III) Chloride | HCID 6451240 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | 1-Indanone, 3-phenyl- | HCID 98146 | 85.4% |
反応手順
To 25.0 g of aluminum chloride, 8.5 g of cinnamic acid and 37.5 ml of benzene were added and the mixture was reacted under reflux for 5 hours. The reaction solution was processed by a usual method to obtain 5.1 g of 3-phenyl-1-indanone.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05721288 |
| 出典データセット | uspto-grants-1998_02 |
| ORD ID | ord-a49f611610274bb892e899afe57aaf15 |
| 出典メモ | uspto-grants-1998_02 |