化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Hydroxide → Leucinamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | Leucinamide hydrochloride | HCID 2733199 | — |
| 溶媒 | Water | HCID 962 | — |
| 溶媒 | Dimethylacetamide | HCID 31374 | — |
| 生成物 | Leucinamide | HCID 69640 | — |
反応手順
1.25M solution of Leu-NH2 in DMAC was prepared by dissolving Leu-NH2.HCl (1.33 g, 7.98 mmol) in 5.0 mL of water, titrating to pH 8.0 with 1M NaOH, lyophilizing, and taking up the residue in 6.4 ml of DMAC. The NaCl precipitate was removed by filtering through a fine glass frit to give a clear solution of pH 9.25.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05563044 |
| 出典データセット | uspto-grants-1996_10 |
| ORD ID | ord-b5d127ef1e6044608b68a102b37d5fbf |
| 出典メモ | uspto-grants-1996_10 |