2-(Dimethylamino)ethanol → Isopropyl 2-dimethylaminoethyl carbonate
反応式
[CH3:1][N:2]([CH2:4][CH2:5][OH:6])[CH3:3].[C:7](=O)([O:10][CH:11]([CH3:13])[CH3:12])[O:8]C>CO>[C:7](=[O:8])([O:6][CH2:5][CH2:4][N:2]([CH3:3])[CH3:1])[O:10][CH:11]([CH3:13])[CH3:12]参加物
4
実験手順
reacting 2-(N,N-dimethylamino)ethanol with the methyl isopropyl carbonate formed in step i) in the presence of a transesterification catalyst to form isopropyl 2-dimethylaminoethyl carbonate and methanol, under such conditions that the 2-(N,N-dimethylamino)ethanol also reacts with the diisopropyl carbonate formed in step i) to form more isopropyl 2-dimethylaminoethyl carbonate,
出典と根拠
- ORDレコード
- ord-dea318db98f74081977ee6eb793bba9f
- 出典データセット
- uspto-grants-1996_10
- 特許番号
- US05563288
反応ノート
読み込み中…