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N,N-dimethyl-5-nitropyridin-2-amine → HCID 178482865、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N,N-dimethyl-5-nitropyridin-2-amine | HCID 75707 | — |
| 反応物 | Diphenyl N-Cyanocarbonimidate | HCID 688090 | — |
| 溶媒 | 1,2-Dimethoxyethane | HCID 8071 | — |
| 生成物 | HCID 178482865 | HCID 178482865 | 74.4% |
反応手順
A stirred mixture of the crude amine prepared from 5.00 g (0.0299 mol) of the product from Step 1, diphenylcyanocarbonimidate (7.20 g, 0.0302 mol) and ethylene glycol dimethyl ether (60 ml) was kept under nitrogen for 3 hours and diluted with Et20. The solid was collected by filtration, washed with Et2O and dried to give 6.26 g of the titled product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05567722 |
| 出典データセット | uspto-grants-1996_10 |
| ORD ID | ord-15d7e9c2f2fb45e3b9b7e58347d30634 |
| 出典メモ | uspto-grants-1996_10 |