関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Benzoguanamine | HCID 7064 | — |
| 反応物 | Nicotinoyl chloride | HCID 82604 | — |
| 溶媒 | Pyridine | HCID 1049 | — |
| 生成物 | 2-Amino-4-nicotinamido-6-phenyl-s-triazine | HCID 14601634 | — |
| 生成物 | 2,4-Bis(nicotinamido)-6-phenyl-s-triazine | HCID 20321035 | — |
反応手順
1.9 g of benzoguanamine and 3.6 g of nicotinic acid chloride (or an equivalent amount of the hydrochloride) are dissolved in 70 ml of pyridine and heated at 60° C for 6 hours. The reaction mixture is processed as described in Example 4 to yield 0.17 g of 2-amino-4-nicotinamido-6-phenyl-s-triazine [mononicotinoylbenzoguanamine] and 1.2 g of 2,4-bis(nicotinamido)-6-phenyl-s-triazine [dinicotinoylbenzoguanamine].
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04098892 |
|---|
| 出典データセット | uspto-grants-1978_07 |
|---|
| ORD ID | ord-181783f4f177426eb5afa527626475a3 |
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| 出典メモ | uspto-grants-1978_07 |
|---|
