関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Nicotinic Acid | HCID 938 | — |
| 反応物 | Benzoguanamine | HCID 7064 | — |
| 反応物 | Chloroethyl carbonate | HCID 22631361 | — |
| 溶媒 | Pyridine | HCID 1049 | — |
| 生成物 | 2,4-Bis(nicotinamido)-6-phenyl-s-triazine | HCID 20321035 | 64.5% |
反応手順
1.9 g of benzoguanamine and 2.6 g of nicotinic acid are dissolved in 50 ml of pyridine and mixed with 2.2 g of chloroethyl carbonate. After heating the mixture at 60° C with agitation for 3 hours, it is processed as described in Example 4 to yield 1.3 g of 2,4-bis(nicotinamido)-6-phenyl-s-triazine [dinicotinoylbenzoguanamine].
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04098892 |
|---|
| 出典データセット | uspto-grants-1978_07 |
|---|
| ORD ID | ord-0822b237088c43928d4831dd80ae9313 |
|---|
| 出典メモ | uspto-grants-1978_07 |
|---|
