関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Nicotinic Acid | HCID 938 | — |
| 反応物 | Benzoguanamine | HCID 7064 | — |
| 反応物 | Methanesulfonyl chloride | HCID 31297 | — |
| 溶媒 | Pyridine | HCID 1049 | — |
| 生成物 | 2-Amino-4-nicotinamido-6-phenyl-s-triazine | HCID 14601634 | — |
| 生成物 | 2,4-Bis(nicotinamido)-6-phenyl-s-triazine | HCID 20321035 | — |
反応手順
1.9 g of benzoguanamine and 2.6 g of nicotinic acid are dissolved in 50 ml of pyridine, and the mixture is further mixed with 2.5 g of methanesulfonyl chloride and agitated at 60° C for 3 hours. Following processing as described in Example 4, there is obtained 0.11 g of 2-amino-4-nicotinamido-6-phenyl-s-triazine [mononicotinoylbenzoguanamine] and 1.05 g of 2,4-bis(nicotinamido)-6-phenyl-s-triazine (dinicotinoylbenzoguanamine).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04098892 |
|---|
| 出典データセット | uspto-grants-1978_07 |
|---|
| ORD ID | ord-ac26d0f05938438796fbe85d5d4447e0 |
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| 出典メモ | uspto-grants-1978_07 |
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