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Iodine → 3-(Cyclohexyldisulfanyl)-2-methylfuran
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Iodine | HCID 807 | — |
| 反応物 | Sodium Carbonate | HCID 10340 | — |
| 反応物 | Cyclohexanethiol | HCID 15290 | — |
| 反応物 | 2-Methyl-3-furanthiol | HCID 34286 | — |
| 溶媒 | Water | HCID 962 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 生成物 | 3-(Cyclohexyldisulfanyl)-2-methylfuran | HCID 20313890 | — |
反応手順
0.57 Grams (0.0050 moles) of 2-methyl-3-furanthiol and 1.16 grams (0.01 moles) of cyclohexylmercaptan are dissolved in 12 ml of diethyl ether. 0.8 Grams (0.0075 moles) of sodium carbonate dissolved in 8 ml water is added to the reaction mass. Over a period of 10 minutes, a solution of 1.9 grams (0.0075 moles) of iodine dissolved in 6 ml diethyl ether is added to the reaction mass with stirring until the iodine color remains. The reaction mass is then stirred over a period of 45 minutes.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04098910 |
| 出典データセット | uspto-grants-1978_07 |
| ORD ID | ord-5bf50225e8f643f8bec01a20944659ad |
| 出典メモ | uspto-grants-1978_07 |