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Dibenzyl sulfide → C6H5CH2SP(S)Cl2
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dibenzyl sulfide | HCID 10867 | — |
| 反応物 | Dioctyl sulfide | HCID 75901 | — |
| 反応物 | n-C8H17SP(S)Cl2 | HCID 15833785 | — |
| 生成物 | C6H5CH2SP(S)Cl2 | HCID 14939050 | 53% |
反応手順
Following the procedure and employing the reaction temperature and reactants of Example 7 with the exception that 53.5 grams (0.25 mole) of (C6H5CH2)2S were employed as a reactant instead of (n-C8H17)2S, 68 grams (53% yield)of C6H5CH2SP(S)Cl2 was obtained. The product had the following properties:
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04100230 |
| 出典データセット | uspto-grants-1978_07 |
| ORD ID | ord-05154d3b49bd4f219f5bcec5a8ff4c21 |
| 出典メモ | uspto-grants-1978_07 |