AGN-PC-0NC49B → HCID 14273353、化合物
反応式
C[O:2][C:3](=[O:5])[O-:4].[CH3:6][N+:7]([CH3:16])([CH3:15])[CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1>O>[C:3](=[O:2])([O-:5])[OH:4].[CH3:6][N+:7]([CH3:16])([CH3:15])[CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1参加物
3
試薬・触媒・溶媒 1
実験手順
112.5 g of trimethylbenzylammonium monomethylcarbonate and 55.0 g of water were introduced in the same reactor as used in Preparation Example 1 and heated with stirring. After the temperature in the reactor reached 120° C., the reaction was continued for 3 hours at 120° C. Trimethylbenzylammonium hydrogencarbonate was obtained in a yield of 95.7 mol %.
後処理
- customas used in Preparation Example 1
- temperatureheated
- customreached 120° C.
出典と根拠
- ORDレコード
- ord-7f7da973e61b4a93aa39d8f9bc886d11
- 出典データセット
- uspto-grants-1988_10
- 特許番号
- US04776929
反応ノート
読み込み中…