HCID 19871551、化合物 → HCID 85570074、化合物
反応式
C[O:2][C:3](=[O:5])[O-:4].[CH3:6][N+:7]([CH3:11])([CH3:10])[CH2:8][CH3:9]>O>[C:3](=[O:2])([O-:5])[OH:4].[CH3:6][N+:7]([CH3:11])([CH3:10])[CH2:8][CH3:9]参加物
3
試薬・触媒・溶媒 1
実験手順
114.1 g of trimethylethylammonium monomethylcarbonate and 75.6 g of water were introduced in the same reactor as used in Preparation Example 1 and heated with stirring. After the temperature in the reactor reached 120° C., the reaction was continued for 3 hours at 120° C. Trimethylethylammonium hydrogencarbonate was obtained in a yield of 96.3 mol %.
後処理
- customas used in Preparation Example 1
- temperatureheated
- customreached 120° C.
出典と根拠
- ORDレコード
- ord-13ae56ff8ff94768903a653a32d808d9
- 出典データセット
- uspto-grants-1988_10
- 特許番号
- US04776929
反応ノート
読み込み中…