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Isatin → 1-[2-(N-isopropylbenzylamino)ethyl]isatin
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Isatin | HCID 7054 | — |
| 反応物 | N-benzyl-N-(2-chloroethyl)propan-2-amine | HCID 48358 | — |
| 生成物 | 1-[2-(N-isopropylbenzylamino)ethyl]isatin | HCID 54367399 | — |
反応手順
By using isatin and the 2-(N-isopropylbenzylamino)ethyl chloride, a method analogous to that described in Reference Example 7 was carried out, and the reaction product was purified with silica gel column chromatography (eluent: chloroform) to obtain 1-[2-(N-isopropylbenzylamino)ethyl]isatin in an oil (yield: 43.4%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04780477 |
| 出典データセット | uspto-grants-1988_10 |
| ORD ID | ord-76f01a9d89844f46acebacb597d71f37 |
| 出典メモ | uspto-grants-1988_10 |