化工社化工社 化学情報印刷レポート · 研究参考用
Acetic Acid → Benzothiophene 1,1-dioxide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetic Acid | HCID 176 | — |
| 反応物 | Hydrogen Peroxide | HCID 784 | — |
| 反応物 | Water | HCID 962 | — |
| 反応物 | Benzo(B)Thiophene | HCID 7221 | — |
| 生成物 | Benzothiophene 1,1-dioxide | HCID 69997 | — |
反応手順
A solution of 40 grams of thianaphthene (Aldrich Chemical Co.), acetic acid (240 ml) and 30% hydrogen peroxide (180 ml) was heated at reflux for 15 minutes. This solution was added to water (800 ml), cooled and filtered to give thianaphthene-1,1-dioxide, m.p.--142°-143° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04780480 |
| 出典データセット | uspto-grants-1988_10 |
| ORD ID | ord-771635f94d434e7dbd7ec22af284e105 |
| 出典メモ | uspto-grants-1988_10 |