Hydrazine → 2,4-Dimethylbenzohydrazide
反応式
[CH3:1][C:2]1[CH:11]=[C:10]([CH3:12])[CH:9]=[CH:8][C:3]=1[C:4](OC)=[O:5].[NH2:13][NH2:14]>CO>[CH3:1][C:2]1[CH:11]=[C:10]([CH3:12])[CH:9]=[CH:8][C:3]=1[C:4]([NH:13][NH2:14])=[O:5]参加物
4
実験手順
To a solution of methyl 2,4-dimethylbenzoate (2 g, 12.2 mmol) in MeOH (10 mL) was added anhydrous hydrazine (1.95 mL, 61 mmol) and the mixture was heated under reflux for 40 hours. Then the mixture was evaporated and dried under vacuum to give 2,4-dimethylbenzohydrazide as a white solid (2 g, 100%; MS (M+H, 165).
後処理
- temperaturethe mixture was heated
- temperatureunder reflux for 40 hours
- customThen the mixture was evaporated
- customdried under vacuum
出典と根拠
- ORDレコード
- ord-f378556826b04b0b900242b1ebc2cb1b
- 出典データセット
- uspto-grants-2015_03
- 特許番号
- US08968708B2
反応ノート
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