化工社化工社 化学情報印刷レポート · 研究参考用
2,3-Dinitrophenol → Sodium dinitrophenolate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,3-Dinitrophenol | HCID 6191 | — |
| 反応物 | Sodium hydride | HCID 24758 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | Sodium dinitrophenolate | HCID 86649331 | — |
反応手順
The anhydrous dinitrophenol (10.0 g, 54.3 mmol) was dissolved in anhydrous THF (300 mL) and then NaH(1.30 g, 54.3 mmol) was added slowly. After the solution was stirred for 3 hrs, solvent was removed under the reduced pressure to obtain 100 mol % sodium dinitrophenolate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08981043B2 |
| 出典データセット | uspto-grants-2015_03 |
| ORD ID | ord-d8af27706dff4fbb87b4281472467d2c |
| 出典メモ | uspto-grants-2015_03 |