化工社化工社 化学情報印刷レポート · 研究参考用
2,3-Dinitrophenol → Sodium dinitrophenolate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,3-Dinitrophenol | HCID 6191 | — |
| 反応物 | Sodium hydride | HCID 24758 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | Sodium dinitrophenolate | HCID 86649331 | — |
反応手順
The anhydrous dinitrophenol (10.0 g, 54.3 mmol) was dissolved in anhydrous THF (300 mL) and then NaH (1.30 g, 54.3 mmol) was added slowly. After the solution was stirred for 3 hrs, solvent was removed under the reduced pressure to obtain 100 mol % sodium dinitrophenolate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08987411B2 |
| 出典データセット | uspto-grants-2015_03 |
| ORD ID | ord-bb64b922e5af466a87709b09e9ad12cb |
| 出典メモ | uspto-grants-2015_03 |