化工社化工社 化学情報印刷レポート · 研究参考用
2-Isopropoxyphenylboronic acid → N-[4-(2-Isopropoxy-phenyl)-pyridin-3-yl]-N-methyl-3,5-bis-trifluoromethyl-benzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Isopropoxyphenylboronic acid | HCID 5084099 | — |
| 反応物 | N-(4-bromo-pyridin-3-yl)-N-methyl-3,5-bis-trifluoromethyl-benzamide | HCID 86670692 | — |
| 生成物 | N-[4-(2-Isopropoxy-phenyl)-pyridin-3-yl]-N-methyl-3,5-bis-trifluoromethyl-benzamide | HCID 60197300 | — |
反応手順
The title compound was prepared in analogy to example 25, from N-(4-bromo-pyridin-3-yl)-N-methyl-3,5-bis-trifluoromethyl-benzamide (example 25, intermediate a) and 2-isopropoxyphenylboronic acid (CAS RN 138008-97-6). Black solid (25%). MS (ESI): m/z=483.0 [M+H]+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08987307B2 |
| 出典データセット | uspto-grants-2015_03 |
| ORD ID | ord-cb5d3a83e72142528684a96edd1bb779 |
| 出典メモ | uspto-grants-2015_03 |