化工社化工社 化学情報印刷レポート · 研究参考用
4-Methyl-3-(trifluoromethyl)benzoic acid → 4,N-Dimethyl-N-(4-o-tolyl-pyridin-3-yl)-3-trifluoromethyl-benzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Methyl-3-(trifluoromethyl)benzoic acid | HCID 2775592 | — |
| 反応物 | N-methyl-4-o-tolylpyridin-3-amine | HCID 18403336 | — |
| 生成物 | 4,N-Dimethyl-N-(4-o-tolyl-pyridin-3-yl)-3-trifluoromethyl-benzamide | HCID 60197696 | — |
反応手順
The title compound was prepared in analogy to example 90, from N-methyl-4-o-tolylpyridin-3-amine (example 1, intermediate a) and 4-methyl-3-trifluoromethyl-benzoic acid (CAS RN 261952-01-6) after a reaction time of 90 hours. Grey solid (32%). MS (ESI): m/z=385.15 [M+H]+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08987307B2 |
| 出典データセット | uspto-grants-2015_03 |
| ORD ID | ord-f0848890fd14425ca24be45b1ff70017 |
| 出典メモ | uspto-grants-2015_03 |