Triethylethylenediamine → (E)-N-(2-(diethylamino)ethyl)-N-ethyl dec-2-enamide

反応式

[C:1]([OH:12])(=O)/[CH:2]=[CH:3]/[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[CH2:13]([NH:15][CH2:16][CH2:17][N:18]([CH2:21][CH3:22])[CH2:19][CH3:20])[CH3:14]>>[CH2:19]([N:18]([CH2:21][CH3:22])[CH2:17][CH2:16][N:15]([CH2:13][CH3:14])[C:1](=[O:12])/[CH:2]=[CH:3]/[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10])[CH3:20]

参加物

反応物 2

HCID 66040Triethylethylenediamine

HCID 5282724trans-2-Decenoic acid

生成物 1

HCID 86694812(E)-N-(2-(diethylamino)ethyl)-N-ethyl dec-2-enamide

実験手順

The same operation as in Example 1-1 or 1-2 was carried out using trans-2-decenoic acid and N,N′,N′-triethylethylenediamine as starting materials to give the aimed compound.

出典と根拠

ORDレコード: ord-5bc28473ddd040ddabb071cc309e49a9
出典データセット: uspto-grants-2015_03
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08987486B2

反応ノート

読み込み中…