化工社化工社 化学情報印刷レポート · 研究参考用
Dichlorobenzyl chloride → 6-bromo-1-(2,3-dichlorobenzyl)-3-methyl-1H-indazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dichlorobenzyl chloride | HCID 76790 | — |
| 反応物 | 1-benzyl-1H-indole-6-carboxylic acid | HCID 17947875 | — |
| 反応物 | HCID 178434209 | HCID 178434209 | — |
| 生成物 | 6-bromo-1-(2,3-dichlorobenzyl)-3-methyl-1H-indazole | HCID 68184280 | 85.5% |
反応手順
The titled compound (228 mg) as a white solid was prepared from the 6-bromo-3-methyl-1H-indazole (152 mg) obtained with the method described in the document (JP 2009-528363 W) and 2,3-dichlorobenzyl chloride (215 mg) according to the method of the process (1) of Example 66.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08987473B2 |
| 出典データセット | uspto-grants-2015_03 |
| ORD ID | ord-3197af0bf3864058b1276d64180ca859 |
| 出典メモ | uspto-grants-2015_03 |