化工社化工社 化学情報印刷レポート · 研究参考用
Triethylamine → Benzyl 4-chlorobenzoyloxycarbamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| 反応物 | Benzyl hydroxycarbamate | HCID 18907 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 生成物 | Benzyl 4-chlorobenzoyloxycarbamate | HCID 51033117 | — |
反応手順
4-Chlorobenzoyl chloride (13.1 mL, 102 mmol) is added slowly to a solution of benzyl hydroxycarbamate (19.0 g, 114 mmol) and triethylamine (14.4 mL, 104 mmol) in diethyl ether (500 mL) at 0° C. then stirred at room temperature for 1 h. The reaction is
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08987504B2 |
| 出典データセット | uspto-grants-2015_03 |
| ORD ID | ord-61ae2cfa3efb4b06b28f8c9207977e98 |
| 出典メモ | uspto-grants-2015_03 |