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2-(Trifluoromethoxy)phenylboronic Acid (contains varying amounts of Anhydride) → 1-Ethyl-4,4,6-trimethyl-7-(2-trifluoromethoxy-phenyl)-3,4-dihydro-1H-quinolin-2-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-(Trifluoromethoxy)phenylboronic Acid (contains varying amounts of Anhydride) | HCID 2777204 | — |
| 反応物 | 7-Bromo-1-ethyl-4,4,6-trimethyl-3,4-dihydro-1H-quinolin-2-one | HCID 21966486 | — |
| 生成物 | 1-Ethyl-4,4,6-trimethyl-7-(2-trifluoromethoxy-phenyl)-3,4-dihydro-1H-quinolin-2-one | HCID 68666393 | — |
反応手順
Compound 9A was prepared from Compound 1A using the procedure described in Example 1B, except using 2-trifluoromethoxy benzene boronic acid as the starting material. MS (electrospray): mass calculated for C21H22F3NO2 377.16; m/z found m/z found, 378.2 [M+H]+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08236819B2 |
| 出典データセット | uspto-grants-2012_08 |
| ORD ID | ord-d90a840a2dbc425bab429a7f289f65f6 |
| 出典メモ | uspto-grants-2012_08 |