化工社化工社 化学情報印刷レポート · 研究参考用
Ethanol → Ethyl 2-(3-hydroxy-4-methoxyphenyl)acetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | 3-Hydroxy-4-methoxybenzeneacetic acid | HCID 160562 | — |
| 生成物 | Ethyl 2-(3-hydroxy-4-methoxyphenyl)acetate | HCID 5324706 | — |
反応手順
To 3-hydroxy-4-methoxyphenylacetic acid (5.0 g, 23.8 mmol) in EtOH (100 mL) was added sulfuric acid (1 mL), and the reaction was stirred overnight at room temperature. Once no starting material was seen by analytical tlc, the mixture was concentrated to give the desired product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08242145B2 |
| 出典データセット | uspto-grants-2012_08 |
| ORD ID | ord-8e44c9051365405ca7c7ab4f06655442 |
| 出典メモ | uspto-grants-2012_08 |