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4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazole → 3-Phenyl-2-[3-(1H-pyrazol-4-yl)-phenyl]-propionitrile
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazole | HCID 2774010 | — |
| 反応物 | 2-(3-Bromo-phenyl)-3-phenyl-propionitrile | HCID 59331981 | — |
| 生成物 | 3-Phenyl-2-[3-(1H-pyrazol-4-yl)-phenyl]-propionitrile | HCID 11300273 | — |
反応手順
2-(3-Bromo-phenyl)-3-phenyl-propionitrile was reacted with 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazole following the procedure set out in Example 1 to give the title compound. (LC/MS: (PS-A) Rt 2.98 [M+H]+ 274).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08247576B2 |
| 出典データセット | uspto-grants-2012_08 |
| ORD ID | ord-bd133740b17844af8e74d3b99062b7c5 |
| 出典メモ | uspto-grants-2012_08 |