Hydrochloric Acid → HCID 68715431、化合物
反応式
C(OC([N:8]1[CH2:13][CH2:12][N:11]([C:14]([CH3:18])([CH3:17])[CH2:15][OH:16])[CH2:10][CH2:9]1)=O)(C)(C)C.[ClH:19]>ClCCl>[ClH:19].[CH3:18][C:14]([N:11]1[CH2:10][CH2:9][NH:8][CH2:13][CH2:12]1)([CH3:17])[CH2:15][OH:16]参加物
4
実験手順
To a solution of 4-(2-hydroxy-1,1-dimethyl-ethyl)-piperazin-1-carboxylic acid tert-butyl ester (0.42 g) in anhydrous dichloromethane (10 mL) was added 2M hydrogen chloride (8.4 ml) and the mixture stirred for 12 hours. The solvent was evaporated to give 2-methyl-2-piperazin-1-yl-propan-1-ol hydrochloride salt as a white solid.
後処理
- customThe solvent was evaporated
出典と根拠
- ORDレコード
- ord-404f1e323d3c4cdc93c81190c7f8947a
- 出典データセット
- uspto-grants-2012_08
- 特許番号
- US08252792B2
反応ノート
読み込み中…