関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Phosgene | HCID 6371 | — |
| 反応物 | 2-Ethylcyclohexan-1-amine | HCID 544854 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 2-Ethylcyclohexylisocyanate | HCID 22250922 | — |
反応手順
To a solution of 2-ethylcyclohexylamine (0.61 mmol) in methanol was added HCl (4.0 M in dioxane, 0.152 mL), and concentrated to give a residue. Phosgene solution (20% in toluene, 6.0 mL) was added, and the reaction was heated at 110° C. overnight. Toluene and excess of phosgene were removed in vacuo to give a residue.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06995269B2 |
|---|
| 出典データセット | uspto-grants-2006_02 |
|---|
| ORD ID | ord-0f7d26ca9bd248889f2a788c0d2faa80 |
|---|
| 出典メモ | uspto-grants-2006_02 |
|---|
