3-Ethylpentane-2,4-dione → 2-[4-(4-Ethyl-3,5-dimethyl-1H-pyrazol-1-yl)phenyl]ethanol
反応式
[CH2:1]([CH:3]([C:7](=O)[CH3:8])[C:4](=O)[CH3:5])[CH3:2].Cl.[NH:11]([C:13]1[CH:18]=[CH:17][C:16]([CH2:19][CH2:20][OH:21])=[CH:15][CH:14]=1)[NH2:12]>>[CH2:1]([C:3]1[C:7]([CH3:8])=[N:12][N:11]([C:13]2[CH:14]=[CH:15][C:16]([CH2:19][CH2:20][OH:21])=[CH:17][CH:18]=2)[C:4]=1[CH3:5])[CH3:2]参加物
3
実験手順
The title compound was prepared according to the procedure described in step 1 of Example 1 from 3-ethyl-2,4-pentanedione and 2-(4-hydrazinophenyl)ethanol hydrochloride: MS (ESI) m/z 245 [M+H]+, 1H-NMR (CDCl3) δ 7.36-7.26 (4H, m), 3.84 (2H, t, J=6.6 Hz), 2.89 (2H, t, J=6.6 Hz), 2.24 (2H, q, J=7.5 Hz), 2.26 (3H, s), 2.22 (3H, s), 1.12 (3H, t, J=7.5 Hz).
出典と根拠
- ORDレコード
- ord-b047a83665744c8cbae0d318ee2a944d
- 出典データセット
- uspto-grants-2006_02
- 特許番号
- US07001917B2
反応ノート
読み込み中…