5-Methyl-2-pyridinesulfonamide → N-[({2-[4-(3,5-Dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethyl}amino)carbonyl]-5-methyl-2-pyridinesulfonamide

関与物質

反応手順

The title compound was prepared according to the procedure described in step 2 of Example 22 from phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate (step 1 of Example 22) and 5-methyl-2-pyridinesulfonamide: 1H-NMR (CDCl3) δ 8.47 (1H, s), 7.90 (1H, d, J=7.9 Hz), 7.73 (1H, d, J=7.9 Hz), 7.47-7.24 (9H, m), 6.68 (1H, br.s), 3.54-3.44 (2H, m), 2.88-2.83 (2H, m), 2.43 (3H, s), 2.33 (3H, s), 2.27 (3H, s).

情報源と証拠