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3-Cyanobenzene-1-sulfonamide → 3-Cyano-N-[({2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethyl}amino)carbonyl]benzenesulfonamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Cyanobenzene-1-sulfonamide | HCID 2808718 | — |
| 反応物 | Phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate | HCID 22244550 | — |
| 生成物 | 3-Cyano-N-[({2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethyl}amino)carbonyl]benzenesulfonamide | HCID 22244590 | — |
反応手順
The title compound was prepared according to the procedure described in step 1 of Example 42 from phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate (step 1 of Example 22) and 3-cyanobenzenesulfonamide: 1H-NMR (CDCl3) δ 8.26-8.21 (2H, m), 7.86 (1H, d, J=7.9 Hz), 7.68 (1H, t, J=7.9 Hz), 7.46-7.20 (9H, m), 6.01 (1H, br.s), 3.48-3.42 (2H, m), 2.84 (2H, t, J=6.3 Hz), 2.32 (3H, s), 2.21 (3H, s).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07001917B2 |
| 出典データセット | uspto-grants-2006_02 |
| ORD ID | ord-b6c1f8304ba8429c9f0c476212bd1d85 |
| 出典メモ | uspto-grants-2006_02 |