3,4-Dimethoxyphenylboronic acid → HCID 22244574、化合物

反応式

I[C:2]1[C:3]([CH3:17])=[N:4][N:5]([C:8]2[CH:13]=[CH:12][C:11]([CH2:14][CH2:15][OH:16])=[CH:10][CH:9]=2)[C:6]=1[CH3:7].[CH3:18][O:19][C:20]1[CH:21]=[C:22](B(O)O)[CH:23]=[CH:24][C:25]=1[O:26][CH3:27]>>[CH3:18][O:19][C:20]1[CH:21]=[C:22]([C:2]2[C:3]([CH3:17])=[N:4][N:5]([C:8]3[CH:13]=[CH:12][C:11]([CH2:14][CH2:15][OH:16])=[CH:10][CH:9]=3)[C:6]=2[CH3:7])[CH:23]=[CH:24][C:25]=1[O:26][CH3:27]

参加物

反応物 2

HCID 27347023,4-Dimethoxyphenylboronic acid

HCID 222445592-[4-(4-Iodo-3,5-dimethyl-1H-pyrazol-1-yl)phenyl]ethanol

生成物 1

HCID 22244574HCID 22244574、化合物

実験手順

The title compound was prepared according to the procedure described in step 1 of Example 12 from 2-[4-(4-iodo-3,5-dimethyl-1H-pyrazol-1-yl)phenyl]ethanol (step 2 of Example 11) and 3,4-dimethoxyphenylboronic acid: MS (ESI) m/z 353 [M+H]+.

出典と根拠

ORDレコード: ord-c2b98995d65944ecbdac4fc1400b098e
出典データセット: uspto-grants-2006_02
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07001917B2

反応ノート

読み込み中…