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HRID 891177作成日:2026年10月26日

Isobutylene → N-(2-methylphenyl)maleimide isobutene

https://huagongshe.com/reaction/891177

反応式

関与物質

役割名称HCID仕込み量
反応物IsobutyleneHCID 8255—
反応物N-2-TolylmaleimideHCID 19989—
反応物NeodecanoateHCID 21225528—
溶媒TolueneHCID 1140—
生成物N-(2-methylphenyl)maleimide isobuteneHCID 69442194—

反応手順

In a one-liter autoclave were charged 400 ml of toluene as a polymerization solvent, 0.001 moles of perbutyl neodecanoate as a polymerization initiator, 0.42 moles of N-(2-methylphenyl)maleimide, and 4.05 moles of isobutene, and the mixture was subjected to polymerization reaction under a polymerization condition at a polymerization temperature of 60° C. for a polymerization time of 5 hours, to obtain N-(2-methylphenyl)maleimide-isobutene alternating copolymer. The thus obtained N-(2-methylphenyl)maleimide-isobutene alternating copolymer had a weight average molecular weight (Mw) (as reduced into standard polystyrene) of 160,000 and a molecular weight distribution (Mw/Mn), which is expressed by [(weight average molecular weight (Mw))/(number average molecular weight (Mn))], of 2.7.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07001967B2
出典データセットuspto-grants-2006_02
ORD IDord-20cd0d7e689248e394b863043ba2525e
出典メモuspto-grants-2006_02