化工社化工社 化学情報印刷レポート · 研究参考用
Glyoxylic Acid → HCID 11259991、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Glyoxylic Acid | HCID 760 | — |
| 反応物 | Borate | HCID 26574 | — |
| 反応物 | (-)-Cystine | HCID 67678 | — |
| 生成物 | HCID 11259991 | HCID 11259991 | — |
反応手順
The alternative route, relying on in solution phase synthesis of an intermediate product starts with addition of a large excess (40 times) of glyoxylic acid to L-cystine in an alkaline borate buffer. The intermediate product was thereafter, after pH manipulations and conductivity adjustment of the reaction mixture, purified with ion exchange chromatography to give N,N,N′,N′-tetrakis (carboxymethyl)-L-cystine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07005071B2 |
| 出典データセット | uspto-grants-2006_02 |
| ORD ID | ord-ce089f0ba7b44eafb0e7bc10f2374c60 |
| 出典メモ | uspto-grants-2006_02 |