化工社化工社 化学情報印刷レポート · 研究参考用
Ammonium Hydroxide → 5-(4-Chlorophenyl)furan-2-carboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ammonium Hydroxide | HCID 14923 | — |
| 反応物 | 5-(4-chlorophenyl)furan-2-carbonyl Chloride | HCID 2771970 | — |
| 生成物 | 5-(4-Chlorophenyl)furan-2-carboxamide | HCID 4780001 | — |
反応手順
To 1000 ml. of cold, stirring NH4OH, 63 g. (0.26 mole) of 5-(p-chlorophenyl)-2-furoyl chloride is added portionwise. The resulting mixture is stirred at ice bath temperature for 15 minutes and then is stored at room temperature for 18 hours. The solid is filtered, is washed with water and is dried at 60 to yield 56 g. (97%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05118708 |
| 出典データセット | uspto-grants-1992_06 |
| ORD ID | ord-a4006aa4880e431ea97cf944de3c6cef |
| 出典メモ | uspto-grants-1992_06 |