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Methanol → 4-(2-Methoxyethyl)phenol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | 4-Hydroxyphenylglyoxal dimethyl acetal | HCID 19788847 | — |
| 生成物 | 4-(2-Methoxyethyl)phenol | HCID 92516 | 47% |
反応手順
The procedure of Example 2 was repeated with a solution of 2.00 g (10.2) mmol) 4-hydroxyphenylglyoxal dimethyl acetal in 10 g methanol containing 0.37 g (10.2 mmol) hydrogen chloride and a 0.20 g dry 10% Pd/C catalyst being reacted with hydrogen gas pressurized at 50 psig at 25° C. A 47% yield of 4-(2'-methoxyethyl)phenol was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05124489 |
| 出典データセット | uspto-grants-1992_06 |
| ORD ID | ord-d12f1b3bc7654c74aa26163577d4b7bc |
| 出典メモ | uspto-grants-1992_06 |