化工社化工社 化学情報印刷レポート · 研究参考用
Formaldehyde → HCID 178470116、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Formaldehyde | HCID 712 | — |
| 反応物 | 1,2,3,4-Tetrahydro-benzo[b]thieno[2,3,c]pyridine-3-carboxylic acid ethyl ester | HCID 19960928 | — |
| 生成物 | HCID 178470116 | HCID 178470116 | — |
反応手順
1-Methyl-1,2,3,4-tetrahydro-benzo[b]thieno[2,3-c]pyridine-3-carboxylic acid ethyl ester was synthesized by following the same procedure as the synthesis of 1,2,3,4-tetrahydro-benzo[b]thieno[2,3-c]pyridine-3-carboxylic acid ethyl ester in Example 1 except that 19.5 g of acetadehyde was used in place of 10.2 ml of formalin in Example 1.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05126448 |
| 出典データセット | uspto-grants-1992_06 |
| ORD ID | ord-cb1478897d3b47028da5b1a01fb108f8 |
| 出典メモ | uspto-grants-1992_06 |