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Ethylenediamine → N-(2-aminoethyl)-1,2,3,4-tetrahydrobenzo[b]thieno[2,3-c]pyridine-3-carboamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethylenediamine | HCID 3301 | — |
| 反応物 | 2-Tert-butoxycarbonyl-1,2,3,4-tetrahydro-benzo[b]thieno[2,3-c]pyridine-3-carboxylic acid | HCID 69959606 | — |
| 生成物 | N-(2-aminoethyl)-1,2,3,4-tetrahydrobenzo[b]thieno[2,3-c]pyridine-3-carboamide | HCID 69959178 | 54% |
反応手順
By following the same procedure as above using 0.32 g of 2-tert-butoxycarbonyl-1,2,3,4-tetrahydrobenzo[b]thieno[2,3-c]pyridine-3-carboxylic acid and ethylenediamine as the starting materials, 0.19 g (yield of 54%) of N-(2-aminoethyl)-1,2,3,4-tetrahydrobenzo[b]thieno[2,3-c]pyridine-3-carboamide.di-hydrochloride was obtained (see Table 9-1, Table 10-1).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05126448 |
| 出典データセット | uspto-grants-1992_06 |
| ORD ID | ord-3ca250e19e0043788808b1b01fc60b0c |
| 出典メモ | uspto-grants-1992_06 |