化工社化工社 化学情報印刷レポート · 研究参考用
2-Butene, 1-bromo-3-methyl- → 2-Methyl-3-(3-methyl-2-butenyl)-2-oxazolinium bromide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Butene, 1-bromo-3-methyl- | HCID 70092 | — |
| 反応物 | 2-Methyl-2-oxazoline | HCID 70713 | — |
| 生成物 | 2-Methyl-3-(3-methyl-2-butenyl)-2-oxazolinium bromide | HCID 20474261 | — |
反応手順
8.5 g (0.1 mol) of 2-methyloxazoline and 14.9 g (0.1 mol) of 3-methyl-2-butenyl bromide (prenyl bromide) were stirred at 20°-25° C. for 2 hours, crystalline, hygroscopic 2-methyl-3-(3-methyl-2-butenyl)-2-oxazolinium bromide being formed in an exothermic reaction.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04283544 |
| 出典データセット | uspto-grants-1981_08 |
| ORD ID | ord-e9edc9b7d8cc40709aff924efede3c88 |
| 出典メモ | uspto-grants-1981_08 |