反応式
[CH2:1](Br)[CH:2]=[C:3]([CH3:5])[CH3:4].[CH3:7][C:8]1[O:9][CH2:10][CH2:11][N:12]=1.[CH3:13][CH2:14][CH2:15][CH2:16][O-:17].[Na+]>C(Cl)Cl.C(O)CCC>[CH2:16]([O:17][C:8]1([CH3:7])[N:12]([CH2:1][CH:2]=[C:3]([CH3:5])[CH3:4])[CH2:11][CH2:10][O:9]1)[CH2:15][CH2:14][CH3:13]参加物
6
実験手順
14.9 g (0.1 mol) of prenyl bromide and 8.5 g (0.1 mol) of 2-methyl-oxazoline were stirred in 50 ml of methylene chloride at 25° C. for 2 hours and the mixture was treated with 0.11 mol of a sodium butylate solution in n-butanol at 40° C. for 1 hour and worked up in the customary manner. 13.4 g (59 mmols, 59%) of 2-butoxy-2-methyl-3-(3-methyl-2-butenyl)-oxazolidine were obtained by distillation at a boiling point 78°-80° C./0.3 mm Hg.
出典と根拠
- ORDレコード
- ord-78e1a38a124c44999ed74f4911a3ef01
- 出典データセット
- uspto-grants-1981_08
- 特許番号
- US04283544
関連ノート
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